مشخصات پژوهش

صفحه نخست /Application of ...
عنوان Application of Pd-2A3HP-MCM-41 to the Suzuki, Heck and Stille coupling reactions and synthesis of 5-substituted 1H-tetrazoles
نوع پژوهش مقاله چاپ‌شده در مجلات علمی
کلیدواژه‌ها Suzuki; Heck; Stille; 5-substituted 1H-tetrazoles; cross-coupling reactions; mesoporous silica; palladium
چکیده An ecofriendly heterogeneous catalyst has been synthesized by anchoring palladium onto the surface of organically modified mesoporous silica. The prepared catalyst was characterized using X-ray diffraction, Fourier transform infrared and energydispersive X-ray spectroscopies, transmission and scanning electron microscopies, inductively coupled plasma and thermogravimetric techniques. The catalyst shows high activity in the Suzuki, Heck and Stille cross-coupling reactions and the synthesis of 5-substituted 1H-tetrazoles from sodium azide (NaN3). These methods have the advantages of high yields, green reaction conditions, simple methodology and easy separation and workup.
پژوهشگران محسن نیکورزم (نفر اول)، آرش قربانی چقامارانی (نفر دوم)، مریم خانمرادی (نفر سوم)