مشخصات پژوهش

صفحه نخست /Synthesis and ...
عنوان Synthesis and characterization of tribenzyl ammonium-tribromide supported on magnetic Fe3O4 nanoparticles: a robust magnetically recoverable catalyst for the oxidative coupling of thiols and oxidation of sulfides
نوع پژوهش مقاله چاپ‌شده در مجلات علمی
کلیدواژه‌ها 2,3‐dihydroquinazolin‐4(1H)‐ones, Cu(II) immobilized on Fe3O4–DETA, magnetic separation, oxidative coupling
چکیده Cu(II) immobilized on Fe3O4–diethylenetriamine was designed as a new, inexpensive and efficient heterogeneous catalyst for the synthesis of 2,3‐dihydroquinazolin‐4(1H)‐ones and the oxidative coupling of thiols. The structure of the nanomagnetic catalyst was comprehensively characterized using Fourier transform infrared spectroscopy, scanning electron microscopy, energy‐dispersive X‐ray spectroscopy, vibrating sample magnetometry, thermogravimetric analysis, X‐ray diffraction and atomic absorption spectroscopy. Simple preparation of the catalyst from commercially available materials, high catalytic activity, simple operation, high yields, use of green solvents, easy magnetic separation and reusability of the catalyst with unaltered activity make our protocol a green and feasible synthetic strategy
پژوهشگران لطفی شیری (نفر اول)، آرش قربانی چقامارانی (نفر دوم)، مصطفی کاظمی (نفر سوم)