مشخصات پژوهش

صفحه نخست /The first report on the ...
عنوان The first report on the preparation of boehmite silica sulfuric acid and its applications in some multicomponent organic reactions
نوع پژوهش مقاله چاپ‌شده در مجلات علمی
کلیدواژه‌ها EFFICIENT SYNTHESIS; IONIC LIQUID; 2,3-DIHYDROQUINAZOLIN-4(1H)-ONE DERIVATIVES; POLYHYDROQUINOLINE DERIVATIVES; RECOVERABLE NANOCATALYST; ULTRASOUND IRRADIATION; MAGNETIC NANOPARTICLE; FUNCTIONALIZED MCM-41; RECYCLABLE CATALYST; FE3O4 NANOPARTICLES
چکیده Boehmite silica sulfuric acid (boehmite-SSA) has been prepared for the first time via an efficient sequential synthetic procedure. Initially, boehmite nanoparticles were prepared, coated by silica, and then reacted with chlorosulfonic acid to obtain boehmite-SSA. A simple, inexpensive, environmentally friendly and efficient procedure for the synthesis of polyhydroquinoline and 2,3-dihydroquinazolin-4(1H)-one derivatives using this compound as an efficient and novel nanocatalyst has been described. Boehmite-SSA is a stable, heterogeneous, cost-effective, easy to handle, and recoverable catalyst and can be reused for several consecutive runs without a significant loss of catalytic activity. Its structure was characterized by FT-IR spectroscopy, thermogravimetric analysis (TGA), powder X-ray diffraction (XRD) and scanning electron microscopy (SEM).
پژوهشگران آرش قربانی چقامارانی (نفر اول)، بهمن طهماسبی (نفر دوم)