مشخصات پژوهش

صفحه نخست /Protection of hydroxy groups ...
عنوان Protection of hydroxy groups as trimethylsilyl ethers using 1,1,1,3,3,3-hexamethyldisilazane (HMDS) catalyzed by poly(4-vinylpyridinium tribromide)
نوع پژوهش مقاله چاپ‌شده در مجلات علمی
کلیدواژه‌ها Poly(4-vinylpyridinium tribromide); Alcohols; Phenols; Protection; Trimethyl-silylation; Hexamethyldisilazane (HMDS); Protecting groups; Silylation
چکیده A very efficient procedure for the protection of alcohols and phenols is presented. The mixture of 1,1,1,3,3,3-hexamethyldisilazane (HMDS) and catalytic amounts of poly(4-vinylpyridinium tribromide) was found to be effective for the trimethylsilylation of alcohols and phenols. Protection reaction is very simple and performs heterogeneously in acetonitrile at room temperature under mild conditions.
پژوهشگران آرش قربانی چقامارانی (نفر اول)، محمد علی زلفی گل (نفر دوم)، مریم حجامی (نفر سوم)، خورشید درویشی (نفر چهارم)، لاله غلام نیا (نفر پنجم)