2025 : 9 : 29

lotfi shiri

Academic rank: Assistant Professor
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Education: PhD.
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Faculty: Basic Science
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Research

Title
Synthesis, Characterization, and Application of CoFe₂O₄@SiO₂@CPTES@Melamine Nanoparticles as a Magnetic Catalyst for the Synthesis of Pyrazole Derivatives
Type
JournalPaper
Keywords
5-Amino-1H-pyrazole-4-carbonitrile,Phenylhydrazine,Malononitrile,benzaldehyde
Year
2024
Journal Journal of Applied Organometallic Chemistry
DOI
Researchers Ammar Radhi Obaid ، lotfi shiri

Abstract

In this work, an efficient procedure for the synthesis of pyrazole derivatives via a one-pot multi-component reaction of phenyl hydrazine, malanonitrile, and various aromatic aldehydes using CoFe2O4@SiO2@CPTES@Melamine as a magnetic nanocatalyst in water under room temperature conditions is reported. This nanocatalyst was synthesized in several steps and identified by various techniques including Fourier-transform infrared (FT-IR), scanning electron microscopy (SEM), energy dispersive X-ray (EDX), thermogravimetric analysis (TGA), X-ray diffraction (XRD), and vibrating sample magnetometer (VSM) techniques. The advantages of using this magnetic nanocatalyst in this research include easy synthesis, efficiency, non-toxicity, high-efficiency product production, short reaction time, and reusability.