2025 : 9 : 29

Mohammad Soleiman-Beigi

Academic rank: Professor
ORCID:
Education: PhD.
ScopusId:
HIndex:
Faculty: Basic Science
Address:
Phone:

Research

Title
Potassium Natural Asphalt Sulfonate (K‐NAS): Synthesis and characterization as a new recyclable solid basic nanocatalyst and its application in the formation of carbon–carbon bonds
Type
JournalPaper
Keywords
nabasic nanocatalyst, Claisen- Schmidt condensation, Knoevenagel condensation, potassium
Year
2020
Journal APPLIED ORGANOMETALLIC CHEMISTRY
DOI
Researchers Mohammad Soleiman-Beigi ، Saeed Falah ، Homa Kohzadi

Abstract

In this research, we synthesized and characterized a new heterogeneous basic nanocatalyst and its catalytic application was studied in the Claisen‐Schmidt and Knoevenagel condensations. In order to prepare this nanocatalyst, first, the Iranian natural asphalt was sulfonated with the concentrated sulfuric acid and then, converted to the potassium natural asphalt sulfonate (K‐NAS). In order to characterization of the nanocatalyst, used of FT‐IR spectroscopy, scanning electron microscopy (SEM), energy dispersive spectroscopy (EDS), X‐ray diffraction (XRD), inductively coupled plasma (ICP) and thermogravimetric analysis (TGA) techniques. This new basic heterogeneous nanocatalyst have advantages such as being eco‐friendly, huge specific surface area, high reactivity and recyclability.